a7b79176-cf84-6dce-e054-002128a47908 English nonGeographicDataset non geographic dataset British Geological Survey +44 115 936 3100 Environmental Science Centre,Keyworth NOTTINGHAM NOTTINGHAMSHIRE NG12 5GG United Kingdom enquiries@bgs.ac.uk pointOfContact 2026-04-05 UK GEMINI 2.3 http://data.bgs.ac.uk/id/dataHolding/13607626 In-situ rock deformation and micron-scale crack network evolution: a high-resolution time-resolved x-ray micro-tomography dataset (NERC Grant NE/R001693/1) 2020-05-12 creation http://data.bgs.ac.uk/id/dataHolding/13607626 This collection comprises two time-series of 3D in-situ synchrotron x-ray microtomography (μCT) volumes showing two Ailsa Craig micro-granite samples (ACfresh02 and ACHT01) undergoing triaxial deformation. These data were collected in-situ at the PSICHE beamline at the SOLEIL synchrotron, Gif-sur-Yvette, France in December 2016 (standard proposal 20160434) and are fully explained in Cartwright-Taylor A., Main, I.G., Butler, I.B., Fusseis, F., Flynn M. and King, A. (in press), Catastrophic failure: how and when? Insights from 4D in-situ x-ray micro-tomography, J. Geophys. Res. Solid Earth. Together, these two time-series show the influence of heterogeneity on the micro-crack network evolution. Ailsa Craig micro-granite is known for being virtually crack-free. One sample (ACfresh02) remained as-received from the quarry until it was deformed, while the second (ACHT01) was slowly heated to 600 degC and then slowly cooled prior to deformation in order to introduce material disorder in the form of a network of nano-scale thermal cracks. Thus these two samples represent two extreme end-members: (i) ACfresh02 with the lowest possible (to our knowledge) natural pre-existing crack density, and so is a relatively homogeneous sample and (ii) ACHT01 with a thermally-induced nano-crack network imprinted over the nominally crack-free microstructure, and therefore has increased heterogeneity relative to ACfresh02. Each 3D μCT volume shows the sub-region of each sample in which the majority of damage was located and has three parts. Part one is reconstructed 16-bit greyscale data. Part two is 8-bit binary data showing individual voids (pores and micro-cracks) in the dataset after segmentation. Part three is 32-bit data showing the local thickness of each void, as in Cartwright-Taylor et al. (in press) Figures 4 and 5. Each part is a zip file containing a sequence of 2D image files (.tif), sequentially numbered according to the depth (in pixels, parallel to the loading axis) at which it lies within the sample volume. File dimensions are in pixels (2D), with an edge length of 2.7 microns. Each zip file is labelled with the sample name, the relevant letter for each 3D volume as given in Cartwright-Taylor et al. (in press) Tables 3 and 4, part 1, 2 or 3 (depending whether the data are greyscale, binary or local thickness respectively), the differential stress (MPa) on the sample, and the associated ram pressure (bar) to link with individual file names. The following convention is used: sample_letter_part_differentialstress_rampressure_datatype. Also included are (i) two spreadsheets (.xlsx), one for each sample, containing processing parameters and the mechanical stress and strain at which each volume was scanned, and (ii) zip files containing .csv files containing measurement data for the labelled voids in each volume. N.B. void label numbers are not consistent between volumes so they can only be used to obtain global statistics, not to track individual voids. Professor Ian Main University of Edinburgh School of Geosciences Grant Institute, The King's Buildings, James Hutton Road Edinburgh EH9 3FE not available originator Professor Ian Main University of Edinburgh School of Geosciences Grant Institute, The King's Buildings, James Hutton Road Edinburgh EH9 3FE not available principalInvestigator Alexis Cartwright-Taylor University of Edinburgh School of GeoSciences Grant Institute, The King's Buildings, James Hutton Road Edinburgh EH9 3FE alexis.cartwright-taylor@ed.ac.uk originator Ian B. Butler University of Edinburgh School of Geosciences Grant Institute, The King's Buildings, James Hutton Road Edinburgh EH9 3FE not available originator Florian Fusseis University of Edinburgh School of GeoSciences Grant Institute, The King's Buildings, James Hutton Road Edinburgh EH9 3FE not available originator Michael Flynn University of Edinburgh School of GeoSciences Grant Institute, The King's Buildings, James Hutton Road Edinburgh EH9 3FE not available originator Andrew King SOLEIL Synchrotron Gif-sur-Yvette France not available originator Enquiries British Geological Survey United Kingdom not available distributor Enquiries British Geological Survey United Kingdom not available pointOfContact notApplicable https://resources.bgs.ac.uk/images/geonetworkThumbs/a7b79176-cf84-6dce-e054-002128a47908.png Geology GEMET - INSPIRE themes, version 1.0 2008-06-01 publication Rock deformation Heterogeneity Compression tests Faulting Granite BGS Thesaurus of Geosciences 2022 revision NGDC Deposited Data Citable Data dataCentre NERC_DDC otherRestrictions licenceOGL Available under the Open Government Licence subject to the following acknowledgement accompanying the reproduced NERC materials "Contains NERC materials ©NERC [year]" otherRestrictions The copyright of materials derived from the British Geological Survey's work is vested in the Natural Environment Research Council [NERC]. No part of this work may be reproduced or transmitted in any form or by any means, or stored in a retrieval system of any nature, without the prior permission of the copyright holder, via the BGS Intellectual Property Rights Manager. Use by customers of information provided by the BGS, is at the customer's own risk. In view of the disparate sources of information at BGS's disposal, including such material donated to BGS, that BGS accepts in good faith as being accurate, the Natural Environment Research Council (NERC) gives no warranty, expressed or implied, as to the quality or accuracy of the information supplied, or to the information's suitability for any use. NERC/BGS accepts no liability whatever in respect of loss, damage, injury or other occurence however caused. Available under the Open Government Licence subject to the following acknowledgement accompanying the reproduced NERC materials "Contains NERC materials ©NERC [year]" English geoscientificInformation 2016-12-17 2016-12-18 Image (TIFF) Comma-separated values (CSV) witheld Microsoft Excel (XLSX) witheld Enquiries British Geological Survey United Kingdom not available distributor https://webapps.bgs.ac.uk/services/ngdc/accessions/index.html#item135665 WWW:DOWNLOAD-1.0-http--download Data download https://doi.org/10.1029/2020JB019642 WWW:LINK-1.0-http--related Published Paper information https://doi.org/10.5285/0dc00069-8da8-474a-8993-b63ef5c25fb8 WWW:LINK-1.0-http--related Citation Information - Digital Object Identifier (DOI) Cartwright-Taylor, A., Main, I.G., Butler, I.B., Fusseis, F., Flynn M. and King, A. (2020): In-situ rock deformation and micron-scale crack network evolution: a high-resolution time-resolved x-ray micro-tomography dataset. British Geological Survey. (Dataset). https://doi.org/10.5285/0dc00069-8da8-474a-8993-b63ef5c25fb8 information nonGeographicDataset non geographic dataset INSPIRE Implementing rules laying down technical arrangements for the interoperability and harmonisation of Geology 2011 publication See the referenced specification false Commission Regulation (EU) No 1089/2010 of 23 November 2010 implementing Directive 2007/2/EC of the European Parliament and of the Council as regards interoperability of spatial data sets and services 2010-12-08 publication See http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2010:323:0011:0102:EN:PDF false The experimental and processing methodology for these data is described fully in Cartwright-Taylor A., Main, I.G., Butler, I.B., Fusseis, F., Flynn M. and King, A. (in press), Catastrophic failure: how and when? Insights from 4D in-situ x-ray micro-tomography, J. Geophys. Res. Solid Earth, . Each sample underwent triaxial deformation at 15 MPa confining pressure in our x-ray transparent rock deformation rig. Details of the rig can be found in Butler, I.B., Fusseis, F., Cartwright-Taylor, A. and Flynn, M. (submitted), Mjölnir: a miniature triaxial rock deformation apparatus for 4D synchrotron x-ray microtomography, J. Synchr. Rad. The samples were loaded to failure at a constant strain rate of 3 x 10^-5 s^-1 in a step-wise manner, with steps decreasing from 20 to 5 MPa as failure approached. At each step the stress was maintained and a μCT volume acquired. Each volume was reconstructed by filtered back projection. The sub-volume of interest was then extracted from each volume, de-noised and down-sampled to 16-bit before segmentation and subsequent analysis.