Geophysical and transport properties of salt rocks during loading and exposed to dissolution (NERC Grant NE/X012751/1)

The dataset gather data from a dual experiment conducted to the study (i) the stress dependence of ultrasonic (elastic) waves and permeability of salt rocks, and (ii) the monitoring of controlled dissolution in an intact halite sample and a cracked (fractured) one. The tests were run in the high-pressure room-temperature (20°C) experimental setup for flow-through tests at the National Oceanography Centre, Southampton (NOCS) (Falcon et al. 2016). The rig consists of a triaxial vessel equipped with (i) ultrasonic sensors that allow measuring P- and S-wave velocities and their attenuation factors using the pulse echo method (McCann and Sothcott, 1992), and (ii) two rigs of electrodes embedded into the rubber sleeve of the pressure vessel for collecting electrical resistivity data that can be used to build up an electrical tomography of the sample (North el al. 2013). The rig has automatic control of both confining and pore pressure (ISCO EX-100D system). For the operating conditions and in homogeneous samples, the bulk electrical resistivity error is <1% for bulk resistivities <100 Ω m, increasing up to 5% with the degree of heterogeneity and above this resistivity value, at frequencies 1–500 Hz (North et al., 2013). Regarding the ultrasonic data, the technique and instrumentation used in this experiment provide velocity precision of ± 0.1% and accuracy of ± 0.3% (95% confidence), and attenuation accuracy of ± 0.1 dB cm-1 within the frequency range 300-1000 kHz (Best, 1992). The dataset presented here show the ultrasonic data at a single frequency of 600 kHz, obtained from Fourier analysis of broadband signals. Permeability to water and to N2 can be both determined with the aid of integrated flowmeters and pore pressure sensors both up- and downstream of the rock sample. The rock samples include: Pre-Cambrian salt (unknown well, Pakistan (source: www.likit.co.uk/)), Cambrian salt (unknown well, Tunguska Basin, Russia), Triassic salt (Arm Hill #1 well, NW Lancashire, UK), and Messinian salt (3A GN3 S02 well, core # 19, near Marianopoli, Sicily). 2.5 cm length, 5 cm diameter core plugs were extracted from precursor rocks, composition estimated by X-ray diffraction analysis, and connected porosity by He-pycnometry. Falcon-Suarez, I., North, L., Amalokwu, K., Best, A., 2016. Integrated geophysical and hydromechanical assessment for CO2 storage: shallow low permeable reservoir sandstones. Geophysical Prospecting 64, 828-847, http://doi.org/10.1111/1365-2478.12396. McCann, C., Sothcott, J., 1992. Laboratory measurements of the seismic properties of sedimentary rocks. Geological Society, London, Special Publications 65, 285-297, https://doi.org/10.1144/gsl.sp.1992.065.01.22. North, L., Best, A.I., Sothcott, J., MacGregor, L., 2013. Laboratory determination of the full electrical resistivity tensor of heterogeneous carbonate rocks at elevated pressures. Geophysical Prospecting 61, 458-470, https://doi.org/10.1111/j.1365-2478.2012.01113.x .

Date (Creation): 2023-08-08

Citation identifier: http://data.bgs.ac.uk/id/dataHolding/13608094

Point of contact

Organisation name	Individual name	Electronic mail address	Role
National Oceanography Centre	Ismael Falcon Suarez	not available	Originator
National Oceanography Centre	Michael Dale	not available	Originator
British Geological Survey	Enquiries	not available	Distributor
British Geological Survey	Enquiries	not available	Point of contact

Maintenance and update frequency: notApplicable

GEMET - INSPIRE themes, version 1.0

Geology

BGS Thesaurus of Geosciences

Underground storage
Dissolution
NGDC Deposited Data
Primary waves
Shear waves
Hydrogen
Rock salt deposits
Permeability
Ultrasonic tests

dataCentre

NGDC Deposited Data

Keywords

NERC_DDC

Access constraints: Other restrictions

Other constraints: restricted

Other constraints: The dataset has been formally approved by BGS for access by external clients under a BGS Digital Data Licence, issued via BGS's IPR Section. The dataset must not be provided to, or be accessible by, an external client until the IPR Section confirms that signed licence documentation is in place. Refer to the IPR Section (DigitalLE@bgs.ac.) if further advice is required.. Constraint applies until 2024-04-01

Use constraints: Other restrictions

Other constraints: The copyright of materials derived from the British Geological Survey's work is vested in the Natural Environment Research Council [NERC]. No part of this work may be reproduced or transmitted in any form or by any means, or stored in a retrieval system of any nature, without the prior permission of the copyright holder, via the BGS Intellectual Property Rights Manager. Use by customers of information provided by the BGS, is at the customer's own risk. In view of the disparate sources of information at BGS's disposal, including such material donated to BGS, that BGS accepts in good faith as being accurate, the Natural Environment Research Council (NERC) gives no warranty, expressed or implied, as to the quality or accuracy of the information supplied, or to the information's suitability for any use. NERC/BGS accepts no liability whatever in respect of loss, damage, injury or other occurence however caused.

Other constraints: There are no restrictions on the use that may be made of the dataset, although an appropriate copyright acknowledgement must be made when any part of the dataset is reproduced. Either no third party data / information is contained in the dataset or BGS has secured written permission from the owner of any third party data / information contained in the dataset to make the dataset freely available without any use constraints - inclusion of any third party data / information will affect the copyright acknowledgement that needs to be made.

Language: English

Topic category

Geoscientific information

Begin date: 2022-05-15

End date: 2023-02-01

Reference System Information

No information provided.

Distribution format

Name	Version
MS Excel

Distributor contact

Organisation name	Individual name	Electronic mail address	Role
British Geological Survey	Enquiries	not available	Distributor

OnLine resource

Protocol	Linkage	Name
	https://doi.org/10.5285/13c05fe8-0d1d-49e5-b55e-5cf4ef241c70	Digital Object Identifier (DOI)

OnLine resource

Protocol	Linkage	Name
	https://webapps.bgs.ac.uk/services/ngdc/accessions/index.html#item181881	Data

Hierarchy level: Non geographic dataset

Other: non geographic dataset

Conformance result

Title: INSPIRE Implementing rules laying down technical arrangements for the interoperability and harmonisation of Geology

Date (Publication): 2011

Explanation: See the referenced specification

Pass: No

Conformance result

Title: Commission Regulation (EU) No 1089/2010 of 23 November 2010 implementing Directive 2007/2/EC of the European Parliament and of the Council as regards interoperability of spatial data sets and services

Date (Publication): 2010-12-08

Explanation: See http://eur-lex.europa.eu/LexUriServ/LexUriServ.do?uri=OJ:L:2010:323:0011:0102:EN:PDF

Pass: No

Statement: For the hydromechanical assessment: hydrostatic confining stress applied following the stress path: 5-10-5-15-5-20-5-30-5-50 MPa. Permeability to N2 and ultrasonic waves were measured at each stress, using the pore pressure transmission technique (e.g., Metwally and Sondergeld, 2011) For the dissolution tests: two samples were exposed to increasing pore pressure up to the constant confining pressure of 16 MPa, while the dissolution process was monitored with ultrasonic waves and electrical resistivity (i.e., decreasing effective stress). Water used for dissolution was a 3.5 wt.% NaCl brine solution Metwally, Y.M., Sondergeld, C.H., 2011. Measuring low permeabilities of gas-sands and shales using a pressure transmission technique. International Journal of Rock Mechanics and Mining Sciences 48, 1135-1144.